4CMX

Crystal structure of Rv3378c

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.3.1
Synchrotron site	ALS
Beamline	8.3.1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	69.460, 94.231, 94.757
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.154 - 2.360
R-factor	0.1695
Rwork	0.164
R-free	0.23880
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	CODE 4CMV
RMSD bond length	0.008
RMSD bond angle	1.116
Data reduction software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.400
High resolution limit [Å]	2.360	2.360
Rmerge	0.130	0.570
Number of reflections	26204
<I/σ(I)>	15.2	2.1
Completeness [%]	100.0	100
Redundancy	4.2	4.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1