4CMW

Crystal structure of Rv3378c

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.3.1
Synchrotron site	ALS
Beamline	8.3.1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	77.165, 101.262, 93.284
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.136 - 2.209
R-factor	0.1796
Rwork	0.177
R-free	0.22940
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4cmv
RMSD bond length	0.009
RMSD bond angle	1.171
Data reduction software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.240
High resolution limit [Å]	2.200	2.200
Rmerge	0.090	0.630
Number of reflections	37194
<I/σ(I)>	18.4	2.3
Completeness [%]	100.0	100
Redundancy	4.2	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1