4C9A
Mouse ZNRF3 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2 (Seleno Met) crystal form I
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-02-22 |
| Detector | DECTRIS PILATUS |
| Spacegroup name | P 1 |
| Unit cell lengths | 36.360, 70.957, 71.994 |
| Unit cell angles | 109.15, 101.71, 101.30 |
Refinement procedure
| Resolution | 38.920 - 2.400 |
| R-factor | 0.19883 |
| Rwork | 0.195 |
| R-free | 0.27293 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.863 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 39.000 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.070 |
| Number of reflections | 19592 |
| <I/σ(I)> | 15 |
| Completeness [%] | 78.5 |
| Redundancy | 6.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
