4C8V
Xenopus RSPO2 Fu1-Fu2 crystal form I
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-08-02 |
| Detector | DECTRIS PILATUS |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 97.138, 97.138, 292.916 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.720 - 2.200 |
| R-factor | 0.22558 |
| Rwork | 0.223 |
| R-free | 0.27035 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.418 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 2.200 |
| Rmerge | 0.110 |
| Number of reflections | 71285 |
| <I/σ(I)> | 10.3 |
| Completeness [%] | 99.1 |
| Redundancy | 6.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
