4C8P

mouse ZNRF3 ectodomain crystal form V, disulfide-bridged S90C variant

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-06-30
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 21 21 2
Unit cell lengths	58.725, 74.297, 38.834
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.070 - 2.100
R-factor	0.20766
Rwork	0.204
R-free	0.28562
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.015
RMSD bond angle	1.846
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.000
High resolution limit [Å]	2.100
Rmerge	0.070
Number of reflections	10421
<I/σ(I)>	11.5
Completeness [%]	99.8
Redundancy	4.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1