4BRP
Legionella pneumophila NTPDase1 crystal form V (part-open)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 129.608, 129.608, 162.698 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.080 - 2.500 |
R-factor | 0.17814 |
Rwork | 0.177 |
R-free | 0.21866 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 1.820 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.090 |
Number of reflections | 55117 |
<I/σ(I)> | 11.8 |
Completeness [%] | 99.9 |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.4 | 100MM NAMES PH 6.4, 14% PEG3350, 200MM KBR |