4BOP
Structure of OTUD1 OTU domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 287 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | I 4 |
Unit cell lengths | 82.240, 82.240, 103.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.672 - 2.100 |
R-factor | 0.1636 |
Rwork | 0.162 |
R-free | 0.20230 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.017 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.970 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.100 | 0.530 |
Number of reflections | 20153 | |
<I/σ(I)> | 8.9 | 2.3 |
Completeness [%] | 96.8 | 97.9 |
Redundancy | 3.2 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10% PEG 4K, 20% GLYCEROL, 0.09M NPS |