4BDZ
PFV intasome with inhibitor XZ-90
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Collection date | 2010-09-18 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 160.170, 160.170, 123.490 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.870 - 2.850 |
| R-factor | 0.18329 |
| Rwork | 0.182 |
| R-free | 0.21477 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 3L2T |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.541 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 3.000 |
| High resolution limit [Å] | 2.850 | 2.850 |
| Rmerge | 0.100 | 0.560 |
| Number of reflections | 35399 | |
| <I/σ(I)> | 8.8 | 2 |
| Completeness [%] | 98.7 | 97.6 |
| Redundancy | 3.7 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | pH 6.5 |
