4B7G
Structure of a bacterial catalase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 63 |
Unit cell lengths | 151.751, 151.751, 157.682 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.802 - 1.900 |
R-factor | 0.135 |
Rwork | 0.133 |
R-free | 0.17430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8cat |
RMSD bond length | 0.008 |
RMSD bond angle | 1.183 |
Data scaling software | SCALEPACK |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.920 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.120 | 0.660 |
Number of reflections | 161469 | |
<I/σ(I)> | 7 | |
Completeness [%] | 99.6 | |
Redundancy | 6.7 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |