4B5I

Product complex of Neisseria AP endonuclease in presence of metal ions

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Spacegroup name	P 43 21 2
Unit cell lengths	69.090, 69.090, 119.670
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.231 - 2.555
R-factor	0.207
Rwork	0.205
R-free	0.25150
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.003
RMSD bond angle	0.536
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	59.800
High resolution limit [Å]	2.550
Rmerge	0.070
Number of reflections	9098
Completeness [%]	99.2
Redundancy	6.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1