4B3L
Family 1 6-phospho-beta-D glycosidase from Streptococcus pyogenes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 120 |
Collection date | 2011-02-04 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 107.830, 198.040, 107.880 |
Unit cell angles | 90.00, 118.51, 90.00 |
Refinement procedure
Resolution | 94.750 - 2.510 |
R-factor | 0.20767 |
Rwork | 0.205 |
R-free | 0.26139 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1od0 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.698 |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0025) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.020 | 2.580 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.050 | 0.510 |
Number of reflections | 134562 | |
<I/σ(I)> | 17 | 2.2 |
Completeness [%] | 99.0 | 100 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M BIS TRIS PROPANE PH 7.5, 20% PEG 3350, 0.2 M NAF |