4AZV

Co-crystal structure of WbdD and kinase inhibitor GW435821x.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	I 2 3
Unit cell lengths	159.320, 159.320, 159.320
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	112.656 - 3.291
R-factor	0.2245
Rwork	0.223
R-free	0.26530
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.356
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	112.800
High resolution limit [Å]	3.240
Rmerge	0.120
Number of reflections	10923
<I/σ(I)>	11.5
Completeness [%]	99.9
Redundancy	5.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1