4AZT

Co-crystal structure of WbdD and kinase inhibitor LY294002.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	I 2 3
Unit cell lengths	158.984, 158.984, 158.984
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	112.420 - 2.340
R-factor	0.19087
Rwork	0.188
R-free	0.25517
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.014
RMSD bond angle	1.784
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	42.500
High resolution limit [Å]	2.340
Rmerge	0.060
Number of reflections	27997
<I/σ(I)>	27.1
Completeness [%]	99.3
Redundancy	8.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1