4AYX
STRUCTURE OF THE HUMAN MITOCHONDRIAL ABC TRANSPORTER, ABCB10 (ROD FORM B)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-07-25 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 180.136, 180.136, 50.565 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.000 - 2.900 |
R-factor | 0.225 |
Rwork | 0.223 |
R-free | 0.26700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ayt |
RMSD bond length | 0.009 |
RMSD bond angle | 0.970 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.000 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.050 | 0.600 |
Number of reflections | 21011 | |
<I/σ(I)> | 13.1 | 1.8 |
Completeness [%] | 99.6 | 99.7 |
Redundancy | 3.4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9.5 | 0.1 M SODIUM CHLORIDE, 0.1 M GLYCINE PH 9.5, 33% (V/V) PEG 300. |