4AXR

CRYSTAL STRUCTURE OF thaumatin FROM A AUTO-HARVESTED CRYSTAL

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 41 21 2
Unit cell lengths	57.976, 57.976, 150.378
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.910 - 1.380
R-factor	0.13604
Rwork	0.134
R-free	0.16565
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.026
RMSD bond angle	2.013
Refinement software	REFMAC (5.6.0116)

Data quality characteristics

	Overall
Low resolution limit [Å]	45.910
High resolution limit [Å]	1.380
Rmerge	0.120
Number of reflections	46257
Completeness [%]	86.0
Redundancy	9.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1