4ATW
The crystal structure of Arabinofuranosidase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 6C1 |
| Synchrotron site | PAL/PLS |
| Beamline | 6C1 |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 210 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 103.710, 161.538, 112.602 |
| Unit cell angles | 90.00, 106.30, 90.00 |
Refinement procedure
| Resolution | 29.940 - 3.000 |
| R-factor | 0.227 |
| Rwork | 0.227 |
| R-free | 0.26200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.100 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.940 | 3.110 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.130 | 0.640 |
| Number of reflections | 60127 | |
| <I/σ(I)> | 14.28 | 2.45 |
| Completeness [%] | 94.0 | 93.1 |
| Redundancy | 6.2 | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 10% PEG 8000, 0.1 M SODIUM CACODYLATE (PH 6.5), 0.2 M MAGNESIUM ACEATE |
