4ATI

MITF:M-box complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Collection date	2009-02-16
Detector	ADSC QUANTUM 315r
Spacegroup name	C 1 2 1
Unit cell lengths	118.990, 104.260, 44.900
Unit cell angles	90.00, 112.15, 90.00

Refinement procedure

Resolution	37.869 - 2.600
R-factor	0.2302
Rwork	0.227
R-free	0.27370
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4ath
RMSD bond length	0.010
RMSD bond angle	1.361
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	55.000	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.050	0.390
Number of reflections	15081
<I/σ(I)>	15.6	3.1
Completeness [%]	96.6	96.6
Redundancy	3.5	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1