4ARR
Crystal structure of the N-terminal domain of Drosophila Toll receptor with the magic triangle I3C
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-01-24 |
| Detector | ADSC QUANTUM 315 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 87.643, 87.643, 220.741 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.700 - 3.000 |
| R-factor | 0.2257 |
| Rwork | 0.224 |
| R-free | 0.25390 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.930 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.400 | 3.160 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.140 | 0.650 |
| Number of reflections | 31669 | |
| <I/σ(I)> | 14.1 | 3.4 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 13 | 12 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | SODIUM MALONATE AND 5-AMINO-2,4, 6-TRIIODOISOPHTHALIC ACID, pH 7 |
