4AQA
CRYSTAL STRUCTURE OF DEAFNESS ASSOCIATED MUTANT MOUSE CADHERIN-23 EC1- 2D124G AND PROTOCADHERIN-15 EC1-2 FORM I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-06-29 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 173.293, 40.506, 84.629 |
Unit cell angles | 90.00, 102.86, 90.00 |
Refinement procedure
Resolution | 34.190 - 1.960 |
R-factor | 0.18035 |
Rwork | 0.178 |
R-free | 0.22775 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4apx |
RMSD bond length | 0.009 |
RMSD bond angle | 1.327 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.190 | 2.000 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmerge | 0.110 | 0.400 |
Number of reflections | 41729 | |
<I/σ(I)> | 8.5 | 2.4 |
Completeness [%] | 99.4 | 95.5 |
Redundancy | 3.4 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.1 MES, 8% PEG 20000, PH 6.5 |