4ANF

Structure of the ornithine carbamoyltransferase from Mycoplasma penetrans with a P23 Space group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-2
Synchrotron site	ESRF
Beamline	ID23-2
Temperature [K]	100
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	P 21 3
Unit cell lengths	167.907, 167.907, 167.907
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.471 - 2.600
R-factor	0.1778
Rwork	0.175
R-free	0.23750
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.185
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.470	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.090	0.370
Number of reflections	47867
<I/σ(I)>	8.7	2.4
Completeness [%]	98.6	95.4
Redundancy	2.4	2.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1