4ALP
The Lin28b Cold shock domain in complex with hexauridine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY |
| Synchrotron site | BESSY |
| Beamline | BL14-1 |
| Temperature [K] | 100 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 95.982, 61.166, 63.219 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 32.420 - 1.480 |
| R-factor | 0.17023 |
| Rwork | 0.169 |
| R-free | 0.18768 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.568 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 32.400 |
| High resolution limit [Å] | 1.480 |
| Rmerge | 0.060 |
| Number of reflections | 60327 |
| <I/σ(I)> | 1 |
| Completeness [%] | 96.2 |
| Redundancy | 6.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
