4AKV

Crystal structure of human sorting nexin 33 (SNX33)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	73
Detector technology	CCD
Collection date	2011-12-14
Detector	ADSC CCD
Spacegroup name	P 21 21 2
Unit cell lengths	68.650, 216.210, 58.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	65.431 - 2.651
R-factor	0.2134
Rwork	0.210
R-free	0.26950
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.002
RMSD bond angle	0.614
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	SHELXD
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	216.140	2.790
High resolution limit [Å]	2.650	2.650
Rmerge	0.100	0.880
Number of reflections	25956
<I/σ(I)>	18.3	2.2
Completeness [%]	100.0	100
Redundancy	10.3	11.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1