4AKG
Dynein Motor Domain - ATP complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-10-23 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 175.326, 117.918, 202.762 |
| Unit cell angles | 90.00, 90.21, 90.00 |
Refinement procedure
| Resolution | 50.000 - 3.300 |
| R-factor | 0.24217 |
| Rwork | 0.239 |
| R-free | 0.30548 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4ai6 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (NULL) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 87.700 | 3.560 |
| High resolution limit [Å] | 3.300 | 3.300 |
| Rmerge | 0.090 | 1.020 |
| Number of reflections | 113780 | |
| <I/σ(I)> | 10.1 | 1.7 |
| Completeness [%] | 96.1 | 86.5 |
| Redundancy | 5.5 | 5.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
