4ADO

Fusidic acid resistance protein FusB

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Spacegroup name	P 1
Unit cell lengths	44.780, 47.310, 53.000
Unit cell angles	89.87, 83.41, 85.66

Refinement procedure

Resolution	27.872 - 2.300
R-factor	0.2066
Rwork	0.204
R-free	0.25430
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.018
RMSD bond angle	1.605
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.000	2.350
High resolution limit [Å]	2.300	2.300
Rmerge	0.070
Number of reflections	18111
<I/σ(I)>	14.38	3.67
Completeness [%]	94.5	95.9
Redundancy	3.86	3.95

Crystallization Conditions

crystal ID	method	pH	temperature	details
1