4AAX
CpGH89CBM32-5, from Clostridium perfringens, in complex with N- acetylgalactosamine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 65.815, 37.268, 57.410 |
| Unit cell angles | 90.00, 103.51, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.900 |
| R-factor | 0.20736 |
| Rwork | 0.204 |
| R-free | 0.26491 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.380 |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.070 |
| Number of reflections | 66214 |
| <I/σ(I)> | 11.6 |
| Completeness [%] | 99.3 |
| Redundancy | 6.14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
