4AAO
MacA-H93G
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-02-08 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 118.719, 118.719, 245.980 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 102.810 - 2.300 |
| R-factor | 0.19223 |
| Rwork | 0.190 |
| R-free | 0.24143 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3hq6 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 2.028 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.6.0113) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.500 | 2.400 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.090 | 0.640 |
| Number of reflections | 45343 | |
| <I/σ(I)> | 20.2 | 3.4 |
| Completeness [%] | 93.5 | 100 |
| Redundancy | 16 | 13.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.4 | 1 M AMMONIUM SULPHATE PH 5.4 |
