4A76
The Lin28b Cold shock domain in complex with heptathymidine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY |
| Synchrotron site | BESSY |
| Beamline | BL14-1 |
| Temperature [K] | 100 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 51.610, 77.575, 100.231 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.880 - 1.920 |
| R-factor | 0.20925 |
| Rwork | 0.207 |
| R-free | 0.24543 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.400 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.900 |
| High resolution limit [Å] | 1.920 |
| Rmerge | 0.070 |
| Number of reflections | 30854 |
| Completeness [%] | 97.9 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
