4A60

Crystal structure of human testis-specific fatty acid binding protein 9 (FABP9)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	CCD
Collection date	2011-08-03
Detector	ADSC CCD
Spacegroup name	P 41 21 2
Unit cell lengths	75.486, 75.486, 113.298
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.600 - 1.530
R-factor	0.1693
Rwork	0.169
R-free	0.18270
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.120
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	BUSTER (2.10.0)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	75.490	1.610
High resolution limit [Å]	1.530	1.530
Rmerge	0.030	0.910
Number of reflections	49689
<I/σ(I)>	18.4	2
Completeness [%]	99.2	98.6
Redundancy	7.5	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1