4A45
CpGH89CBM32-5, from Clostridium perfringens, in complex with GalNAc- beta-1,3-galactose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU-MSC R-AXIS IV++ |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 33.803, 58.631, 70.658 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.130 - 1.750 |
| R-factor | 0.20089 |
| Rwork | 0.199 |
| R-free | 0.24571 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.716 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.750 |
| Rmerge | 0.060 |
| Number of reflections | 14448 |
| <I/σ(I)> | 10.7 |
| Completeness [%] | 97.9 |
| Redundancy | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
