4A44

CpGH89CBM32-5, from Clostridium perfringens, in complex with the Tn Antigen

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Detector technology	IMAGE PLATE
Detector	RIGAKU-MSC R-AXIS IV++
Spacegroup name	P 21 21 21
Unit cell lengths	31.800, 59.260, 67.430
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.500 - 1.700
R-factor	0.18937
Rwork	0.188
R-free	0.22249
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.012
RMSD bond angle	1.801
Data reduction software	d*TREK
Data scaling software	d*TREK
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.700
Rmerge	0.060
Number of reflections	14287
<I/σ(I)>	12
Completeness [%]	97.5
Redundancy	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1