4A42

CpGH89CBM32-6 produced by Clostridium perfringens

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-2
Synchrotron site	SSRL
Beamline	BL9-2
Temperature [K]	100
Detector technology	CCD
Detector	MARMOSAIC 325 mm CCD
Spacegroup name	P 43
Unit cell lengths	48.810, 48.810, 98.180
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.234 - 1.550
R-factor	0.1988
Rwork	0.197
R-free	0.23870
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.011
RMSD bond angle	1.294
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	SHARP
Refinement software	PHENIX ((PHENIX.REFINE: 1.7_650))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.630
High resolution limit [Å]	1.550	1.550
Rmerge	0.050	0.380
Number of reflections	33037
<I/σ(I)>	30.6	7.6
Completeness [%]	99.2	100
Redundancy	15.2	7.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1