4A41
CpGH89CBM32-5, from Clostridium perfringens, in complex with galactose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-002 |
| Temperature [K] | 113 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU-MSC R-AXIS IV++ |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 65.271, 38.322, 53.875 |
| Unit cell angles | 90.00, 90.64, 90.00 |
Refinement procedure
| Resolution | 54.230 - 1.550 |
| R-factor | 0.18831 |
| Rwork | 0.186 |
| R-free | 0.22406 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.415 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.550 |
| Rmerge | 0.060 |
| Number of reflections | 21421 |
| <I/σ(I)> | 13 |
| Completeness [%] | 99.6 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
