4A34
Crystal structure of the fucose mutarotase in complex with L-fucose from Streptococcus pneumoniae
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Detector | RIGAKU AREA DETECTOR |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.319, 144.158, 165.460 |
| Unit cell angles | 90.00, 97.51, 90.00 |
Refinement procedure
| Resolution | 19.970 - 2.500 |
| R-factor | 0.22822 |
| Rwork | 0.225 |
| R-free | 0.29174 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.198 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.500 |
| Rmerge | 0.090 |
| Number of reflections | 97486 |
| Completeness [%] | 99.7 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
