401D
STRUCTURE OF A DNA IN LOW SALT CONDITIONS D(GACCGCGGTC)
Experimental procedure
| Detector technology | AREA DETECTOR |
| Detector | SIEMENS HI-STAR |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 38.444, 38.444, 80.175 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 5.000 - 2.200 |
| R-factor | 0.219 |
| Rwork | 0.219 |
| R-free | 0.28500 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.810 |
| Data reduction software | SAINT |
| Data scaling software | SAINT |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.200 |
| Rmerge | 0.039 |
| Number of reflections | 1811 |
| Completeness [%] | 82.3 |
| Redundancy | 6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | This particular structure is not described in this paper. * |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | SPERMINE_HCL | ||
| 4 | 1 | 1 | NA CACODYLATE | ||
| 5 | 1 | 2 | WATER | ||
| 6 | 1 | 2 | MPD |
