3VWX
Structural analysis of an epsilon-class glutathione S-transferase from housefly, Musca domestica
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2009-01-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 31 |
格子定数 [Å] | 87.548, 87.548, 131.883 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 65.820 - 1.800 |
R因子 | 0.16532 |
Rwork | 0.164 |
R-free | 0.19052 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jlv |
結合長の平均二乗偏差(RMSD) [Å] | 0.022 |
結合角の平均二乗偏差(RMSD) [度] | 1.719 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 75.800 | 1.900 |
分解能 [Å] (高) | 1.800 | 1.800 |
独立反射数 | 102983 | |
完全性 [%] | 98.3 | 97.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.2 M sodium citrate, 0.1 M HEPES-NaOH pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |