3TEN
Holo form of carbon disulfide hydrolase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2008-01-01 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97178 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 204.950, 113.240, 87.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.600 |
R-factor | 0.2675 |
Rwork | 0.266 |
R-free | 0.29922 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.131 | 0.463 |
Number of reflections | 63162 | |
Completeness [%] | 99.5 | 99.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 293 | 25% PEG 1000 200 mM LiCl 50 mM phosphate/citrate buffer , pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K |