3T2C
Fructose-1,6-bisphosphate aldolase/phosphatase from Thermoproteus neutrophilus, DHAP-bound form
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2010-08-01 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | I 4 2 2 |
格子定数 [Å] | 112.348, 112.348, 150.915 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 17.338 - 1.300 |
R因子 | 0.10861 |
Rwork | 0.108 |
R-free | 0.12938 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3t2b |
結合長の平均二乗偏差(RMSD) [Å] | 0.030 |
結合角の平均二乗偏差(RMSD) [度] | 2.572 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 17.338 | 1.330 |
分解能 [Å] (高) | 1.300 | 1.300 |
Rmerge_l_obs | 0.066 | 0.373 |
独立反射数 | 117471 | |
<I/σ(I)> | 17.4 | 4.9 |
完全性 [%] | 99.8 | 99.9 |
冗長性 | 7.9 | 7.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 294 | 8% PEG3350, 0.1 M HEPES/NaOH, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |