3KYS
Crystal structure of human YAP and TEAD complex
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-06 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.97869 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 44.643, 110.503, 165.695 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 40.160 - 2.800 |
R因子 | 0.2296 |
Rwork | 0.228 |
R-free | 0.26580 |
Structure solution method | SAD |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX (1.18.2_3874) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.900 |
分解能 [Å] (高) | 2.800 | 2.800 |
Rmerge_l_obs | 0.063 | 0.354 |
独立反射数 | 20593 | 20593 |
<I/σ(I)> | 44.3 | 3.91 |
完全性 [%] | 97.9 | 83.6 |
冗長性 | 13.8 | 10.1 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 277 | 0.1M sodium acetate, 2M sodium formate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 277K |