3GBI
The Rational Design and Structural Analysis of a Self-Assembled Three-Dimensional DNA Crystal
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Detector technology | CCD |
Collection date | 2008-06-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | H 3 |
格子定数 [Å] | 107.161, 107.161, 93.144 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 17.288 - 4.018 |
R因子 | 0.246 |
Rwork | 0.240 |
R-free | 0.30900 |
結合長の平均二乗偏差(RMSD) [Å] | 0.016 |
結合角の平均二乗偏差(RMSD) [度] | 1.364 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL2Map |
Refinement software | PHENIX |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 17.300 | 4.070 |
分解能 [Å] (高) | 4.010 | 4.000 |
Rmerge_l_obs | 0.067 | |
独立反射数 | 3211 | |
<I/σ(I)> | 10.9 | |
完全性 [%] | 96.1 | 100 |
冗長性 | 7.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | Grown by vapor diffusion while treated with a controlled temperature gradient from 333 degs to 293 degs., pH 8.5, VAPOR DIFFUSION, SITTING DROP |