3FK3
Structure of the Yeats Domain, Yaf9
Experimental procedure
実験手法 | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2004-06-15 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.11587, 0.9795, 1.0199 |
Spacegroup name | P 65 2 2 |
格子定数 [Å] | 84.725, 84.725, 288.212 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 20.000 - 2.300 |
R因子 | 0.22394 |
Rwork | 0.222 |
R-free | 0.25746 |
Structure solution method | MAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
結合角の平均二乗偏差(RMSD) [度] | 0.989 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.000 | 2.420 |
分解能 [Å] (高) | 2.300 | 2.300 |
独立反射数 | 24936 | |
完全性 [%] | 95.8 | 92.8 |
冗長性 | 6.3 | 5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | MICROBATCH | 7.5 | 291 | 10% PEG 3350, 100 mM Na, Tartrate, 20% glycerol, pH 7.5, microbatch, temperature 291K |