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3FA6

Crystal structure of the R132K:Y134F:R111L:L121D:T54V mutant of cellular retinoic acid-binding protein II complexed with C15-aldehyde (a retinal analog) at 1.54 angstrom resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 21-ID-D
Synchrotron siteAPS
Beamline21-ID-D
Temperature [K]100
Detector technologyCCD
Collection date2007-08-08
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)0.97869
Spacegroup nameP 21 21 21
Unit cell lengths37.261, 89.634, 90.621
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution32.160 - 1.540
R-factor0.17388
Rwork0.171
R-free0.22055
RMSD bond length0.014
RMSD bond angle1.623
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]63.7601.600
High resolution limit [Å]1.5401.540
Rmerge0.0540.366
Number of reflections45260
<I/σ(I)>31.32.5
Completeness [%]98.796.7
Redundancy4.63.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.82770.1M sodium acetate, 18% PEG6000, pH 5.8, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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數據於2024-09-18公開中

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