Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-10-29 |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 31 2 1 |
格子定数 [Å] | 83.010, 83.010, 162.979 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 50.000 - 2.300 |
R因子 | 0.22 |
Rwork | 0.220 |
R-free | 0.26000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ihm |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | |
分解能 [Å] (高) | 2.300 | 2.300 |
独立反射数 | 23678 | |
冗長性 | 3.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 295 | 13% (w/v) PEG 4000, 0.2 M (NH4)2SO4, 0. 1 M NaOAc, pH 4.50, VAPOR DIFFUSION, HANGING DROP, temperature 295K |