3ZY2
Crystal structure of POFUT1 in complex with GDP (High resolution dataset)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM16 |
| Synchrotron site | ESRF |
| Beamline | BM16 |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 145.018, 38.247, 68.196 |
| Unit cell angles | 90.00, 103.07, 90.00 |
Refinement procedure
| Resolution | 70.630 - 1.540 |
| R-factor | 0.2057 |
| Rwork | 0.205 |
| R-free | 0.23725 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.373 |
| Data reduction software | XDS |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.500 | 1.620 |
| High resolution limit [Å] | 1.540 | 1.540 |
| Rmerge | 0.040 | 0.280 |
| Number of reflections | 53812 | |
| <I/σ(I)> | 20.8 | 4.8 |
| Completeness [%] | 99.1 | 99.7 |
| Redundancy | 4.1 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
