3ZVQ

Crystal Structure of proteolyzed lysozyme

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	298
Detector technology	IMAGE PLATE
Detector	MARRESEARCH
Spacegroup name	P 43 21 2
Unit cell lengths	78.558, 78.558, 38.216
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	24.840 - 2.000
R-factor	0.2131
Rwork	0.213
R-free	0.23750
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	193l
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS (1.3)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	24.840
High resolution limit [Å]	2.000	2.000
Rmerge	0.100	0.380
Number of reflections	7699
Completeness [%]	93.9	90.4
Redundancy	4.5	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1			298	20MG/ML PROTEOLYZED LYSOZYME, 15%PEG3500, 25C