3ZQV

RECOMBINANT NATIVE CYTOCHROME C PRIME FROM ALCALIGENES XYLOSOXIDANS AT 0.84 A RESOLUTION: NON-RESTRAINED REFINEMENT

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2008-04-07
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 65 2 2
Unit cell lengths	53.470, 53.470, 181.190
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 0.840
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.043
RMSD bond angle	2.764
Data reduction software	XDS
Data scaling software	XDS
Refinement software	SHELXL-97

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.000	0.900
High resolution limit [Å]	0.840	0.840
Rmerge	0.040	0.780
Number of reflections	128930
<I/σ(I)>	10.5	2.12
Completeness [%]	92.2	72.8
Redundancy	6	5.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		AMMONIUM SULPHATE, PH 7.5