3ZQP
Crystal structure of the small terminase oligomerization domain from a SPP1-like bacteriophage
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Collection date | 2004-02-04 |
| Spacegroup name | P 32 |
| Unit cell lengths | 74.271, 74.271, 119.632 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 25.000 - 3.000 |
| R-factor | 0.18714 |
| Rwork | 0.185 |
| R-free | 0.22592 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3zqm |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.241 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0116) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.800 | 3.160 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.110 | 0.370 |
| Number of reflections | 14792 | |
| <I/σ(I)> | 7 | 2.7 |
| Completeness [%] | 98.1 | 96.8 |
| Redundancy | 4.1 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.2 M MGCL2, 8% PEG 550MME, 0.1 M TRIS PH 8.0 |
