3ZPE
Structure of the carboxy-terminal domain of the turkey type 3 siadenovirus fibre
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-10-26 |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 98.570, 98.570, 98.570 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 28.510 - 2.200 |
| R-factor | 0.20101 |
| Rwork | 0.199 |
| R-free | 0.24155 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.506 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.320 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.090 | 0.690 |
| Number of reflections | 8256 | |
| <I/σ(I)> | 17.5 | 3.8 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 11.6 | 12 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | 25 MM MORPHOLINO-ETHANESULFONIC ACID, 0.5-1.0 M DIAMMONIUM PHOSPHATE, 0.1 M SODIUM CITRATE PH 5.5-5.8, 0.2-0.3 M SODIUM CHLORIDE |
