3ZOR
Structure of BsUDG
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2010-06-05 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 65.305, 79.795, 97.362 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.730 - 2.950 |
| R-factor | 0.24045 |
| Rwork | 0.238 |
| R-free | 0.29516 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3zoq CHAIN A |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.739 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.980 | 3.110 |
| High resolution limit [Å] | 2.950 | 2.950 |
| Rmerge | 0.160 | 0.460 |
| Number of reflections | 5596 | |
| <I/σ(I)> | 8.5 | 3.4 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 6.1 | 6.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 291 | 0.2 M SODIUM FLUORIDE AND 20% PEG 3350 AT 291 K, pH 7.5 |
