3ZO7

Crystal structure of ClcFE27A with substrate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	77.836, 103.112, 137.767
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.935 - 2.224
R-factor	0.1872
Rwork	0.186
R-free	0.23240
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.947
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.360
High resolution limit [Å]	2.220	2.220
Rmerge	0.050	0.470
Number of reflections	102684
<I/σ(I)>	13.6	2.04
Completeness [%]	97.6	91.2
Redundancy	4.7	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1