3ZNT

Crystal structure of OXA-24 class D beta-lactamase with tazobactam

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	CCD
Collection date	2012-09-23
Detector	ADSC QUANTUM 315r
Spacegroup name	P 41 21 2
Unit cell lengths	102.898, 102.898, 86.344
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.020 - 1.950
R-factor	0.18294
Rwork	0.182
R-free	0.20934
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3g4p
RMSD bond length	0.012
RMSD bond angle	1.436
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.000	2.060
High resolution limit [Å]	1.950	1.950
Rmerge	0.070	0.510
Number of reflections	34412
<I/σ(I)>	25.5	7
Completeness [%]	100.0	100
Redundancy	17.6	17.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1