3ZNT
Crystal structure of OXA-24 class D beta-lactamase with tazobactam
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-23 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 102.898, 102.898, 86.344 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.020 - 1.950 |
R-factor | 0.18294 |
Rwork | 0.182 |
R-free | 0.20934 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3g4p |
RMSD bond length | 0.012 |
RMSD bond angle | 1.436 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.000 | 2.060 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.070 | 0.510 |
Number of reflections | 34412 | |
<I/σ(I)> | 25.5 | 7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 17.6 | 17.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |